Synthetic and Electrochemical Studies of [2Fe2S] Complexes Containing a 4-Amino-1,2-dithiolane-4-carboxylic Acid Moiety

Author(s)
Ulf-Peter Apfel, Christian Kowol, Enrico Morera, Helmar Görls, Gino Lucente, Bernhard Keppler, Wolfgang Weigand
Abstract

In the search for novel [FeFe] hydrogenase model systems several di and tripeptides containing an 4 amino 1 2-dithiolane 4 carboxylic acid (Adt) moiety or N-phenylsulfonyl Adt OMe were treated with Fe-3(CO)(12) The resulting [FeFe] complexes were characterized by H-1 and C-13 NMR spectroscopy, mass spectrometry and elemental analysis All complexes were investigated by cyclic voltammetry, and their ability to catalyze the reduction of protons to dihydrogen, as a function of acid concentration, was studied in different solvents

Organisation(s)
Department of Inorganic Chemistry
External organisation(s)
Friedrich-Schiller-Universität Jena, Sapienza University of Rome
Journal
European Journal of Inorganic Chemistry
Volume
32
Pages
5079-5086
No. of pages
8
ISSN
1434-1948
DOI
https://doi.org/10.1002/ejic.201000619
Publication date
2010
Peer reviewed
Yes
Austrian Fields of Science 2012
104003 Inorganic chemistry
Portal url
https://ucrisportal.univie.ac.at/en/publications/2b4d3567-6122-47c4-84d0-befd43a6c291