G-quadruplex vs. duplex-DNA binding of nickel(II) and zinc(II) Schiff base complexes

Author(s)
Riccardo Bonsignore, Alessio Terenzi, Angelo Spinello, Annamaria Martorana, Antonino Lauria, Anna Maria Almerico, Bernhard K. Keppler, Giampaolo Barone
Abstract

Novel nickel(II) (1) and zinc(II) (2) complexes of a Salen-like ligand, carrying a pyrimidine ring on the N,N′ bridge, were synthesized and characterized. Their interaction with duplex and G-quadruplex DNA was investigated in aqueous solution through UV-visible absorption, circular dichroism and viscometry measurements. The results obtained point out that, while the zinc(II) complex does not interact with both duplex and G-quadruplex DNA, the nickel(II) complex 1 binds preferentially to G-quadruplex respect to duplex-DNA, with values of the DNA-binding constants, K

b, 2.6 × 10

5 M

- 1 and 3.5 × 10

4 M

- 1, respectively. Molecular dynamics simulations provided an atomic level model of the top-stacking binding occurring between 1 and hTelo (a 22-mer sequence oligonucleotide) in G-quadruplex conformation.

Organisation(s)
Department of Inorganic Chemistry
External organisation(s)
Università degli Studi di Palermo, Istituto Euro-Mediterraneo di Scienza e Tecnologia (IEMEST), Medizinische Universität Wien
Journal
Journal of Inorganic Biochemistry
Volume
161
Pages
115-121
No. of pages
7
ISSN
0162-0134
DOI
https://doi.org/10.1016/j.jinorgbio.2016.05.010
Publication date
08-2016
Peer reviewed
Yes
Austrian Fields of Science 2012
104003 Inorganic chemistry, 106002 Biochemistry
Keywords
ASJC Scopus subject areas
Biochemistry, Inorganic Chemistry
Portal url
https://ucrisportal.univie.ac.at/en/publications/375cafcf-600b-49d2-88ee-00f19eea33d8